HRID1888968

反应详情

EQUATION

反应方程式

REACTANTS

反应物

反应SMILES：CC(C)=N[C@H](C(=O)N1[C@H](C#N)C[C@@H]2C[C@@H]21)C12CC3CC(CC(O)(C3)C1)C2

HCID54577999

未命名化合物

PRODUCTS

产物

反应SMILES：N#C[C@@H]1C[C@@H]2C[C@@H]2N1C(=O)[C@@H](N)C12CC3CC(CC(O)(C3)C1)C2.O

HCID53297473

未命名化合物

收率 80.1%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID962

Water

H2O

PROCEDURE

实验过程

The Schiff base (Compound M, 7.27 g) was suspended in 25 ml of water. The obtained suspension was stirred overnight at room temperature in a closed flask. The product was filtered off and dried at 40° C./0 mbar for 2 hours. (Yield=80.1%) HPLC 100%, Powder XRD—H-1

WORKUP

后处理

filtrationThe product was filtered off
customdried at 40° C./0 mbar for 2 hours