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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1888968Generated: October 29, 2026

HCID 54577999, compound → Saxagliptin Hydrate

https://huagongshe.com/reaction/1888968

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 54577999HCID 54577999—
SolventWaterHCID 962—
ProductSaxagliptin HydrateHCID 5329747380.1%

Reaction Steps

The Schiff base (Compound M, 7.27 g) was suspended in 25 ml of water. The obtained suspension was stirred overnight at room temperature in a closed flask. The product was filtered off and dried at 40° C./0 mbar for 2 hours. (Yield=80.1%) HPLC 100%, Powder XRD—H-1

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08501960B2
Source datasetuspto-grants-2013_08
ORD IDord-46d92c5e6b264fd7a7d91d3fa5859288
Source noteuspto-grants-2013_08