HuagongsheHuagongshe Chemistry Print Report · For research reference only
10-Bromodecanoic Acid → 10-Azidodecanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 10-Bromodecanoic Acid | HCID 142712 | — |
| Reactant | 9-Azidononanoic acid | HCID 15230549 | — |
| Product | 10-Azidodecanoic acid | HCID 85714144 | 91% |
Reaction Steps
10-bromodecanoic acid (1.125 gr, 4.48 mmol) was reacted as described for product 5a to yield 91% of product 5b. 1H-NMR (200 MHz, CDCl3): 1.2-1.5 (m; 10H), 1.5-1.7 (m; 4H), 2.35 (t; J=7.41 Hz; 2H), 3.24 (t; J=6.81 Hz; 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08501969B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-c8b9509ab73e4d29b28c94e1bc43e34b |
| Source note | uspto-grants-2013_08 |