HuagongsheHuagongshe Chemistry Print Report · For research reference only
Fluorosulfuric acid → HCID 86644015, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Fluorosulfuric acid | HCID 24603 | — |
| Reactant | Tricyclohexylphosphine | HCID 75806 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 86644015 | HCID 86644015 | 105.1% |
Reaction Steps
0.7 ml (12 mmol) fluorosulfonic acid is added to 25 ml of a solution of 12 mmol tricyclohexyl phosphine in diethylether prepared as in example 2. The product precipitates with a strong exotherm. 4.8 g of a colorless solid is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08501985B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-00439bd6162e462b8174b336196f289f |
| Source note | uspto-grants-2013_08 |