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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1889416Generated: November 1, 2026

HCID 59351564, compound → HCID 59351494, compound

https://huagongshe.com/reaction/1889416

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 59351564HCID 59351564—
CatalystHCID 178418390HCID 178418390—
SolventTetrahydrofurfuryl alcoholHCID 7360—
ProductHCID 59351494HCID 5935149478%

Reaction Steps

To a solution (20 mL) of 3-(2-phenylethyl)-6-vinylquinazoline-2,4(1H,3H)-dione (0.6 g) in tetrahydrofuran-methanol (1:1) was added palladium carbon (10%, 0.06 g), and the mixture was stirred under hydrogen atmosphere for 4 hr. Insoluble material was filtered off, and the filtrate was concentrated to give the title compound as a brown solid (0.47 g, 78%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08501750B2
Source datasetuspto-grants-2013_08
ORD IDord-96f698878ed341e287926045708611b4
Source noteuspto-grants-2013_08