HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2,4-Dichlorophenyl)boronic acid → HCID 178515770, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2,4-Dichlorophenyl)boronic acid | HCID 2734659 | — |
| Reactant | HCID 178420377 | HCID 178420377 | — |
| Product | HCID 178515770 | HCID 178515770 | — |
Reaction Steps
From 5-(benzyloxy)-3H-imidazo[4,5-b]pyridine and 2,4-dichlorophenylboronic acid, prepared in a similar manner as the one described in Example 1.26, the title compound was obtained. LCMS m/z=279.9 [M+H]+; 1H NMR (400 MHz, methanol-d4) δ ppm 6.72 (d, J=8.7 Hz, 1H), 7.57 (dd, J1=8.5 Hz, J2=2.2 Hz, 1H), 7.63 (d, J=8.5 Hz, 1H), 7.79 (d, J=2.2 Hz, 1H), 7.99 (d, J=8.7 Hz, 1H), 8.34 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08507473B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-687d384e50754a31aa830cff3773256e |
| Source note | uspto-grants-2013_08 |