HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-2-fluorophenylboronic Acid → HCID 178515769, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-2-fluorophenylboronic Acid | HCID 16217158 | — |
| Reactant | HCID 178420377 | HCID 178420377 | — |
| Product | HCID 178515769 | HCID 178515769 | — |
Reaction Steps
From 5-(benzyloxy)-3H-imidazo[4,5-b]pyridine and 3-chloro-2-fluorophenylboronic acid, prepared in a similar manner as the one described in Example 1.26, the title compound was obtained. LCMS m/z=263.9 [M+H]+; 1H NMR (400 MHz, methanol-d4) δ ppm 6.73 (d, J=8.7 Hz, 1H), 7.39 (td, J1=8.2 Hz, J2=1.5 Hz, 1H), 7.68 (m, 2H), 8.00 (d, J=8.7 Hz, 1H), 8.36 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08507473B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-9b317766ce8e4f4cade738b1729f67a5 |
| Source note | uspto-grants-2013_08 |