4-Ethylaniline → HCID 43330298, compound

HRID 1890327Notes

Reaction equation

HRID 1890327 reaction equation
Cl[C:2]1[C:7]([N+:8]([O-:10])=[O:9])=[CH:6][CH:5]=[C:4]([Cl:11])[N:3]=1.[CH2:12]([C:14]1[CH:20]=[CH:19][C:17]([NH2:18])=[CH:16][CH:15]=1)[CH3:13]>>[Cl:11][C:4]1[N:3]=[C:2]([NH:18][C:17]2[CH:19]=[CH:20][C:14]([CH2:12][CH3:13])=[CH:15][CH:16]=2)[C:7]([N+:8]([O-:10])=[O:9])=[CH:6][CH:5]=1

Participants

3

Reactant 2

HCID 115044-EthylanilineHCID 852392,6-Dichloro-3-nitropyridine

Product 1

HCID 43330298HCID 43330298, compound

Procedure

From 2,6-dichloro-3-nitropyridine and 4-ethylaniline, prepared in a similar manner as the one described in Example 1.21 with the exception that the reaction was performed at 65° C., the title compound was obtained.

Workup

  1. customwas performed at 65° C.

Sources & evidence

ORD record
ord-31778343881d482f8dcff559c28d2f6d
Source dataset
uspto-grants-2013_08
Patent number
US08507473B2

Reaction notes

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