O-Toluidine → HCID 43330246, compound

HRID 1890362Notes

Reaction equation

HRID 1890362 reaction equation
Cl[C:2]1[C:7]([N+:8]([O-:10])=[O:9])=[CH:6][CH:5]=[C:4]([Cl:11])[N:3]=1.[NH2:12][C:13]1[C:14]([CH3:19])=[CH:15][CH:16]=[CH:17][CH:18]=1>>[Cl:11][C:4]1[N:3]=[C:2]([NH:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=2[CH3:19])[C:7]([N+:8]([O-:10])=[O:9])=[CH:6][CH:5]=1

Participants

3

Reactant 2

HCID 7242O-ToluidineHCID 852392,6-Dichloro-3-nitropyridine

Product 1

HCID 43330246HCID 43330246, compound

Procedure

From 2,6-dichloro-3-nitropyridine and o-toluidine, prepared in a similar manner as the one described in Example 1.127, Step A, the title compound was obtained. LCMS m/z=264.30 [M+H]+.

Sources & evidence

ORD record
ord-c95bdc97a0bf431a91a6fdf7160b22fb
Source dataset
uspto-grants-2013_08
Patent number
US08507473B2

Reaction notes

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