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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1890425Generated: November 1, 2026

2,4-Dimethoxybenzoic acid → HCID 44176533, compound

https://huagongshe.com/reaction/1890425

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2,4-Dimethoxybenzoic acidHCID 7052—
Reactant4-Chloro-o-anisic acidHCID 93682—
ReactantHCID 66841894HCID 66841894—
ProductHCID 44176533HCID 44176533—

Reaction Steps

By analogy with the method described in example 1 (step 1.8), using 9-amino-4-oxo-2-pyridin-4-yl-5,6,8,9-tetrahydro-4H-1,4a,7-triaza-benzocycloheptene-7-carboxylic acid ethyl ester and 2,4-dimethoxy-benzoic acid in place of (+/−)-9-amino-4-oxo-2-pyrimidin-4-yl-5,6,8,9-tetrahydro-4H-1,4a,7-triaza benzocycloheptene-7-carboxylic acid ethyl ester hydrobromide (1:1) and 4-chloro-2-methoxy-benzoic acid, the compound, 0.103 g (76%), was obtained as a white powder.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08507476B2
Source datasetuspto-grants-2013_08
ORD IDord-4e7bc9a4669d4734973838c8fcde1f72
Source noteuspto-grants-2013_08