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HRID1890437

反应详情

EQUATION

反应方程式

HRID 1890437 的结构方程式

REACTANTS

反应物

2
结构：COc1ccc2ncc(=O)[nH]c2c1
HCID491319

7-Methoxyquinoxalin-2(1H)-one

C9H8N2O2

结构：CC(C)(C)OC(=O)N1CC(COS(C)(=O)=O)C1
HCID21959416

tert-Butyl 3-{[(methanesulfonyl)oxy]methyl}azetidine-1-carboxylate

C10H19NO5S

PRODUCTS

生成物

1
结构：COc1ccc2ncc(=O)n(CC3CN(C(=O)OC(C)(C)C)C3)c2c1
HCID67130867

未命名化合物

收率 35.7%

PROCEDURE

实验过程

Using the procedure of Example 2, step 2.i, but starting from 7-methoxy-2(1H)-quinoxalinone (1.00 g; prepared according to WO 2006/134378) and 3-[[(methylsulfonyl)oxy]methyl]-1-azetidinecarboxylic acid tert-butyl ester (1.65 g; prepared according to WO 02/066470), the second eluting compound was isolated as a yellow oil (700 mg, 35% yield).