HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 67305098, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | thieno[3,2-b]pyridin-2-ylmethanol | HCID 13220437 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67305098 | HCID 67305098 | — |
Reaction Steps
To a solution of thieno[3,2-b]pyridin-2-ylmethanol (C-4) (17 mg, 0.1 mmol) in anhydrous dichloromethane (10 mL) was added SOCl2 (120 mg). After the mixture was stirred at room temperature for 2 hours, it was concentrated and used for the next step without further purification. MS (m/z): 184 (M+1)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08507487B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-11a18eba2cf64383a2ca13b696238e4a |
| Source note | uspto-grants-2013_08 |