HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58550526, compound → HCID 136127571, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58550526 | HCID 58550526 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 136127571 | HCID 136127571 | — |
Reaction Steps
A mixture of [6-(2-benzyloxy-phenyl)-pyrimidin-4-yl]-(3-methanesulfonyl-phenyl)-amine (7.90 g, 18.3 mmol) and trifluoroacetic acid (100 mL) was refluxed to completion of the reaction. All the volatiles were evaporated in vacuo, the residue was re-crystallized from ethanol to give 2-[6-(3-methanesulfonyl-phenylamino)-pyrimidin-4-yl]-phenol as white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08507498B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-310f3a075ee143579160989b91826256 |
| Source note | uspto-grants-2013_08 |