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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1890986Generated: October 31, 2026

HCID 58550526, compound → HCID 136127571, compound

https://huagongshe.com/reaction/1890986

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 58550526HCID 58550526—
SolventTrifluoroacetic acidHCID 6422—
ProductHCID 136127571HCID 136127571—

Reaction Steps

A mixture of [6-(2-benzyloxy-phenyl)-pyrimidin-4-yl]-(3-methanesulfonyl-phenyl)-amine (7.90 g, 18.3 mmol) and trifluoroacetic acid (100 mL) was refluxed to completion of the reaction. All the volatiles were evaporated in vacuo, the residue was re-crystallized from ethanol to give 2-[6-(3-methanesulfonyl-phenylamino)-pyrimidin-4-yl]-phenol as white powder.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08507498B2
Source datasetuspto-grants-2013_08
ORD IDord-310f3a075ee143579160989b91826256
Source noteuspto-grants-2013_08