2-Amino-6-methoxybenzothiazole → N-(6-Methoxybenzo[d]thiazol-2-yl)-1H-imidazole-1-carbothioamide

Participants

Reaction Conditions

Reaction Steps

To 6-methoxybenzo[d]thiazol-2-amine (0.53 g, 2.94 mmol) in acetonitrile (20 mL) was added 1,1′-thiocarbonyldiimidazole (0.681 g, 3.82 mmol). The reaction mixture was stirred at 65° C. for 24 hours. The precipitate was filtered and washed with acetonitrile (2×20 mL) to yield the product. The product was taken directly to the next step without any further purification or characterization.

Provenance & Evidence