反应详情

温度

65 °C

To 6-methoxybenzo[d]thiazol-2-amine (0.53 g, 2.94 mmol) in acetonitrile (20 mL) was added 1,1′-thiocarbonyldiimidazole (0.681 g, 3.82 mmol). The reaction mixture was stirred at 65° C. for 24 hours. The precipitate was filtered and washed with acetonitrile (2×20 mL) to yield the product. The product was taken directly to the next step without any further purification or characterization.

1. filtrationThe precipitate was filtered
2. washwashed with acetonitrile (2×20 mL)
3. customto yield the product
4. customThe product was taken directly to the next step without any further purification or characterization