HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 60130838, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | 3-Aminopyrrolidine | HCID 164401 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 60130838 | HCID 60130838 | 60.3% |
Reaction Steps
Benzaldehyde (21.2 g; 0.20 mol) was added, dropwise, to a solution of 3-aminopyrrolidine (17.2 g; 0.20 mol) in toluene (80 ml). The solution thus obtained was stirred at room temperature. After 3 h the solvent was removed by evaporation at reduced pressure and the residue was taken up twice with toluene. 21 g N-(phenylmethylene)pyrrolidine-3-amine was thus obtained, and was used in subsequent reactions without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08507528B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-4cde63631a6b4a34aa2ccb4e5ca4a9f9 |
| Source note | uspto-grants-2013_08 |