Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1891308Generated: October 31, 2026

Benzaldehyde → HCID 60130838, compound

https://huagongshe.com/reaction/1891308

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzaldehydeHCID 240—
Reactant3-AminopyrrolidineHCID 164401—
SolventTolueneHCID 1140—
ProductHCID 60130838HCID 6013083860.3%

Reaction Steps

Benzaldehyde (21.2 g; 0.20 mol) was added, dropwise, to a solution of 3-aminopyrrolidine (17.2 g; 0.20 mol) in toluene (80 ml). The solution thus obtained was stirred at room temperature. After 3 h the solvent was removed by evaporation at reduced pressure and the residue was taken up twice with toluene. 21 g N-(phenylmethylene)pyrrolidine-3-amine was thus obtained, and was used in subsequent reactions without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08507528B2
Source datasetuspto-grants-2013_08
ORD IDord-4cde63631a6b4a34aa2ccb4e5ca4a9f9
Source noteuspto-grants-2013_08