Boron tribromide → HCID 25152881, compound

Participants

Reaction Steps

The product from step c) (0.6 g) in DCM (10 mL) was treated with 1.0 M boron tribromide in DCM (5 mL) and the reaction was stirred at rt overnight. The reaction was diluted with DCM and washed with ice water, dried (MgSO4) and concentrated under reduced pressure to give the sub titled product as a solid (0.5 g).

Provenance & Evidence