HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCl MTBD
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 7-Methyl-1,5,7-triazabicyclo[4.4.0]dec-5-ene | HCID 123583 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCl MTBD | HCID 131730803 | — |
Reaction Steps
A flame dried flask was charged with MTBD (0.25 g, 1.63 mmol), ether (10 mL) and a stirbar under dry nitrogen atmosphere. With vigorous stirring a 1M ethereal HCl solution (1.6 mL) was then added to form a white precipitate. Stirring was continued for 1 hour then excess solvent was decanted to yield 0.29 g (94%). The salt was then dried under high vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08507640B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-6cd5d35aca5b4ce79e9dae5ea4099b85 |
| Source note | uspto-grants-2013_08 |