HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(4-Isopropylphenyl)butanoic acid → HCID 59409743, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(4-Isopropylphenyl)butanoic acid | HCID 347674 | — |
| Catalyst | Adams' catalyst | HCID 345198 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 59409743 | HCID 59409743 | 107.9% |
Reaction Steps
A suspension of compound 77 (1.0 g, 4.8 mmol) and 0.1 g of PtO2 in 50 mL of acetic acid was stirred under a H2 atmosphere (50 psi) at ambient temperature for 6 hours. After filtering and evaporating off the solvent, 1.1 g crude product was obtained. The compound was used directly in the next step without further purification. LC-MS m/z 211 (M−H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08507647B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-fc6f5632061a4f348c6ca76e3648c2a0 |
| Source note | uspto-grants-2013_08 |