反应详情

温度

70 °C

Diphenyl sulfamoylcarbonimidate, from step A, (0.05 g, 0.17 mmol) and 3-bromoaniline (18 μl, 0.17 mmol) were dissolved in acetonitrile (0.5 ml) and heated to 70° C. for 12 hours. The reaction was concentrated under vacuum to afford phenyl N-3-bromophenyl-N′-sulfamoylcarbamimidate, which was carried on crude to the next reaction.

1. concentrationThe reaction was concentrated under vacuum