Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 3-Bromoaniline | HCID 11562 | — |
| Reactant | Diphenyl sulfamoylcarbonimidate | HCID 15599173 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 68729453 | HCID 68729453 | — |
Reaction Steps
Diphenyl sulfamoylcarbonimidate, from step A, (0.05 g, 0.17 mmol) and 3-bromoaniline (18 μl, 0.17 mmol) were dissolved in acetonitrile (0.5 ml) and heated to 70° C. for 12 hours. The reaction was concentrated under vacuum to afford phenyl N-3-bromophenyl-N′-sulfamoylcarbamimidate, which was carried on crude to the next reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08507672B2 |
|---|
| Source dataset | uspto-grants-2013_08 |
|---|
| ORD ID | ord-432ff1f5c71147a5b241435db4187179 |
|---|
| Source note | uspto-grants-2013_08 |
|---|
