HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 44439950, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | 4-Chlorobenzenesulfonamide | HCID 66824 | — |
| Reactant | 2-Benzyl-3-[(tert-butoxycarbonyl)amino]propanoic acid | HCID 22614206 | — |
| Product | HCID 44439950 | HCID 44439950 | — |
Reaction Steps
N-(tert-butoxycarbonyl)-2-benzyl-β-alanine synthesized by using benzaldehyde as the starting material for the similar procedure as in Reference Examples 2 to 5, Reference Example 23, and Reference Example 33 was used instead of the starting material of Reference Example 148, that is, the compound S33, and 4-chlorobenzenesulfonamide was used instead of 4-nitrobenzenesulfonamide for the similar procedure as in Reference Example 148 to Reference Example 150 and Example 173 to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08507714B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-7bab5b0041d745edbfa0bf162c032ae3 |
| Source note | uspto-grants-2013_08 |