Aniline → HCID 57671118, compound

HRID 1892866Notes

Reaction equation

HRID 1892866 reaction equation
[CH2:1]([CH:8]1[CH2:14][N:13]([CH2:15][CH2:16][C:17]([NH:19]C2C=CC=CC=2)=[O:18])[C:12](=[O:26])[CH2:11][N:10]([S:27]([C:30]2[CH:35]=[CH:34][C:33]([Cl:36])=[CH:32][CH:31]=2)(=[O:29])=[O:28])[C:9]1=[O:37])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.NC1C=CC=CC=1.C[Si](C)(C)N[Si](C)(C)C>>[CH2:1]([CH:8]1[CH2:14][N:13]([CH2:15][CH2:16][C:17]([NH2:19])=[O:18])[C:12](=[O:26])[CH2:11][N:10]([S:27]([C:30]2[CH:31]=[CH:32][C:33]([Cl:36])=[CH:34][CH:35]=2)(=[O:29])=[O:28])[C:9]1=[O:37])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

4

Reactant 3

HCID 6115AnilineHCID 13838HexamethyldisilazaneHCID 57671104HCID 57671104, compound

Product 1

HCID 57671118HCID 57671118, compound

Procedure

Instead of the starting material compound of Example 273, that is, aniline, 1,1,1,3,3,3-hexamethyldisilazane was used for the similar procedure as in Example 273 to obtain the title compound.

Sources & evidence

ORD record
ord-b4832281b0c441089b453310437b1658
Source dataset
uspto-grants-2013_08
Patent number
US08507714B2

Reaction notes

Loading…