HuagongsheHuagongshe Chemistry Print Report · For research reference only
11-Aminoundecanoic acid → N,N,N-Trimethylmethanaminium 11-aminoundecanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 11-Aminoundecanoic acid | HCID 17083 | — |
| Reactant | Tetramethylammonium hydroxide | HCID 60966 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | N,N,N-Trimethylmethanaminium 11-aminoundecanoate | HCID 16212873 | — |
Reaction Steps
Tetramethylammonium 11-aminoundecanoate was synthesized by titration of a methanolic suspension of 11-aminoundecanoic acid (4.04 grams (g) in approximately 4 ml methanol, Aldrich) with methanolic tetramethylammonium hydroxide (8.4 ml, Aldrich), evaporation of the solvent under reduced pressure, and recrystallization from tetrahydrofuran (about 50 ml, Aldrich).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08512946B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-18781f1e58f548db8c82f63860fdca8d |
| Source note | uspto-grants-2013_08 |