huagongshe.com
HRID1893156

反应详情

EQUATION

反应方程式

HRID 1893156 的结构方程式

REACTANTS

反应物

1
结构：CC1(C)OCC(C2OC3OC(C)(C)OC3C2OCc2ccccc2)O1
HCID97907

未命名化合物

PRODUCTS

生成物

1
结构：CC1(C)OC2OC(C(O)CO)C(OCc3ccccc3)C2O1
HCID249093

3-O-Benzyl-1,2-O-isopropylidene-a-D-glucofuranose

C16H22O6

收率 80%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)O
溶剂HCID176

Acetic Acid

C2H4O2

PROCEDURE

实验过程

To a flask charged with 6-Benzyloxy-5-(2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxole was added 75% aqueous solution of acetic acid. The reaction was stirred, extracted, washed, dried and the solvent was evaporated to provide the titled compound in 80% yield.

WORKUP

后处理

  1. extractionextracted
  2. washwashed
  3. customdried
  4. customthe solvent was evaporated