HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-O-Benzyl-1,2:5,6-di-O-isopropylidene-alpha-D-glucofuranose → 3-O-Benzyl-1,2-O-isopropylidene-a-D-glucofuranose
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-O-Benzyl-1,2:5,6-di-O-isopropylidene-alpha-D-glucofuranose | HCID 97907 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 3-O-Benzyl-1,2-O-isopropylidene-a-D-glucofuranose | HCID 249093 | 80% |
Reaction Steps
To a flask charged with 6-Benzyloxy-5-(2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxole was added 75% aqueous solution of acetic acid. The reaction was stirred, extracted, washed, dried and the solvent was evaporated to provide the titled compound in 80% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08513214B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-d6478b0920ae44b7b10c7448e26b9700 |
| Source note | uspto-grants-2013_08 |