4-Bromotoluene → HCID 21350651, compound

HRID 1893287Notes

Reaction equation

Br[C:2]1[CH:7]=[CH:6][C:5]([CH3:8])=[CH:4][CH:3]=1.[O:9]1[C:13]2([CH2:18][CH2:17][C:16](=[O:19])[CH2:15][CH2:14]2)[O:12][CH2:11][CH2:10]1>>[C:5]1([CH3:8])[CH:6]=[CH:7][C:2]([C:16]2([OH:19])[CH2:15][CH2:14][C:13]3([O:12][CH2:11][CH2:10][O:9]3)[CH2:18][CH2:17]2)=[CH:3][CH:4]=1

Participants

Reactant 2

HCID 78054-Bromotoluene

HCID 5674151,4-Dioxaspiro[4.5]decan-8-one

Product 1

HCID 21350651HCID 21350651, compound

Procedure

The title compound was prepared as a white solid from 4-bromotoluene (Aldrich) and 1,4-dioxa-spiro[4.5]decan-8-one using the procedure described in Step A of Example 1.

Sources & evidence

ORD record: ord-2a160cbe23eb4e69906446ff1bb5ba2f
Source dataset: uspto-grants-2013_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08513229B2

Reaction notes

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