HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-bromo-3-methyl-3H-benzooxazol-2-one → 5-(8-Hydroxy-1,4-dioxa-spiro[4.5]dec-8-yl)-3-methyl-3H-benzooxazol-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-bromo-3-methyl-3H-benzooxazol-2-one | HCID 337469 | — |
| Reactant | 1,4-Dioxaspiro[4.5]decan-8-one | HCID 567415 | — |
| Product | 5-(8-Hydroxy-1,4-dioxa-spiro[4.5]dec-8-yl)-3-methyl-3H-benzooxazol-2-one | HCID 59541987 | — |
Reaction Steps
The title compound was prepared as a white solid from 5-bromo-3-methyl-3H-benzooxazol-2-one (prepared by methylation of 5-bromo-3H-benzooxazol-2-one from Aldrich) and 1,4-dioxa-spiro[4.5]decan-8-one using the procedure described in Step A of Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08513229B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-4990443ea434419899e8a3922e822692 |
| Source note | uspto-grants-2013_08 |