HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(1,4-dioxaspiro[4.5]dec-8-ylidene)-2-methylpropane-2-sulfinamide → HCID 20453324, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(1,4-dioxaspiro[4.5]dec-8-ylidene)-2-methylpropane-2-sulfinamide | HCID 59733754 | — |
| Reactant | HCID 178490745 | HCID 178490745 | — |
| Product | HCID 20453324 | HCID 20453324 | — |
Reaction Steps
The title compound was prepared as a white solid from addition of 3-methoxy-phenyl magnesium bromide (Aldrich) to 2-methyl-propane-2-sulfinic acid (1,4-dioxa-spiro[4.5]dec-8-ylidene)-amide (as prepared in Example 84, Step A) followed by hydrolysis using the procedure described in Step B of Example 84.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08513229B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-2ad7bfd22f71430eba26489a07483e5b |
| Source note | uspto-grants-2013_08 |