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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1893519Generated: October 31, 2026

HCID 13673632, compound → HCID 66881270, compound

https://huagongshe.com/reaction/1893519

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 13673632HCID 13673632—
Reactant1,4-Dioxane hydrochlorideHCID 20443148—
SolventDiethyl EtherHCID 3283—
ProductHCID 66881270HCID 6688127053%

Reaction Steps

A pale-yellow oil obtained using the compound (1.20 g, 9.5 mmol) obtained in step A and according to the method of Reference Example 37, step C was dissolved in diethyl ether (15 ml), 4N hydrochloric acid-dioxane solution (1.8 ml) was added with stirring under ice-cooling, and the solution was concentrated under reduced pressure to give the title compound (0.85 g, yield 53%) as a pale-yellow oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08513235B2
Source datasetuspto-grants-2013_08
ORD IDord-9667eb0d54384e42a42c3b3d6418c1bf
Source noteuspto-grants-2013_08