HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13673632, compound → HCID 66881270, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13673632 | HCID 13673632 | — |
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 66881270 | HCID 66881270 | 53% |
Reaction Steps
A pale-yellow oil obtained using the compound (1.20 g, 9.5 mmol) obtained in step A and according to the method of Reference Example 37, step C was dissolved in diethyl ether (15 ml), 4N hydrochloric acid-dioxane solution (1.8 ml) was added with stirring under ice-cooling, and the solution was concentrated under reduced pressure to give the title compound (0.85 g, yield 53%) as a pale-yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08513235B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-9667eb0d54384e42a42c3b3d6418c1bf |
| Source note | uspto-grants-2013_08 |