Iodoethane → HCID 66880526, compound

HRID 1893556Notes

Reaction equation

HRID 1893556 reaction equation
[CH2:1]([O:3][C:4]([C:6]1[CH:7]=[C:8]2[C:13](=[CH:14][C:15]=1[CH3:16])[NH:12][C:11](=[O:17])[CH2:10][CH2:9]2)=[O:5])[CH3:2].[CH2:18](I)[CH3:19]>>[CH2:1]([O:3][C:4]([C:6]1[CH:7]=[C:8]2[C:13](=[CH:14][C:15]=1[CH3:16])[N:12]([CH2:18][CH3:19])[C:11](=[O:17])[CH2:10][CH2:9]2)=[O:5])[CH3:2]

Participants

3

Reactant 2

HCID 6340IodoethaneHCID 66880713HCID 66880713, compound

Product 1

HCID 66880526HCID 66880526, compoundYield 85.1%

Procedure

Using the compound (10.0 g, 42.9 mmol) obtained in step B and ethyl iodide (6.86 ml, 85.8 mmol), and according to the method of Reference Example 113, step B, the title compound (9.54 g, yield 85%) was obtained as a colorless solid.

Sources & evidence

ORD record
ord-5ea37a4c076f4b98a3367ec146ff9d5b
Source dataset
uspto-grants-2013_08
Patent number
US08513235B2

Reaction notes

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