HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylethylamine → HCID 123242916, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | 2-Bromoethylamine hydrobromide | HCID 2774217 | — |
| Reactant | HCID 66880943 | HCID 66880943 | — |
| Product | HCID 123242916 | HCID 123242916 | 70% |
Reaction Steps
Using the compound (1.24 g, 2.85 mmol) of Example 15, step A, 2-bromoethylamine hydrobromide (786 mg, 3.84 mmol), and N,N-diisopropylethylamine (0.70 ml, 4.1 mmol), and according to the method of Example 1, step B, the title compound (1.08 g, yield 70%) was obtained as a colorless solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08513235B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-6a6558df8db34996a7ef0440490eadf2 |
| Source note | uspto-grants-2013_08 |