HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2-Difluoroethyl trifluoromethanesulfonate → HCID 66882345, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2-Difluoroethyl trifluoromethanesulfonate | HCID 2774089 | — |
| Reactant | HCID 66881861 | HCID 66881861 | — |
| Product | HCID 66882345 | HCID 66882345 | 70.3% |
Reaction Steps
Using the compound (767 mg, 1.82 mmol) of Example 241, step B and 2,2-difluoroethyl trifluoromethanesulfonate (534 mg, 2.49 mmol), and according to the method of Example 241, step C, the title compound (621 mg, yield 70%) was obtained as a colorless amorphous solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08513235B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-3beabebf65114ee4942bbe9f24ad02b5 |
| Source note | uspto-grants-2013_08 |