HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2-Difluoroethyl trifluoromethanesulfonate → HCID 66881261, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2-Difluoroethyl trifluoromethanesulfonate | HCID 2774089 | — |
| Reactant | HCID 66896863 | HCID 66896863 | — |
| Product | HCID 66881261 | HCID 66881261 | 68.1% |
Reaction Steps
Using the compound (1.25 g, 2.97 mmol) of Example 257, step B and 2,2-difluoroethyl trifluoromethanesulfonate (859 mg, 4.01 mmol), and according to the method of Example 241, step C, the title compound (982 mg, yield 68%) was obtained as a colorless amorphous solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08513235B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-824d0bb3ec1d464d9749eaabd43af04c |
| Source note | uspto-grants-2013_08 |