HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylsulfamate → Sulfamic acid 1-trifluoroethyl-cyclopropyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylsulfamate | HCID 11030308 | — |
| Reactant | 1-(2,2,2-Trifluoroethyl)cyclopropan-1-ol | HCID 57445153 | — |
| Product | Sulfamic acid 1-trifluoroethyl-cyclopropyl ester | HCID 57785491 | — |
Reaction Steps
Sulfamic acid 1-trifluoroethyl-cyclopropyl ester was synthesized according to the method presented in the synthesis of sulfamic acid phenyl ester in Example 1 with the exception of utilizing 1-trifluoroethylcyclopropanol (synthesized by methods reported in Synthesis 1991, 234.) to obtain sulfamic acid 1-trifluoroethyl-cyclopropyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08513186B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-4ec91c2276e2487bb403e8facabb0875 |
| Source note | uspto-grants-2013_08 |