HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)aniline → HCID 59277819, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)aniline | HCID 2734655 | — |
| Reactant | 2-Bromo-1-methyl-1H-imidazole | HCID 2773262 | — |
| Product | HCID 59277819 | HCID 59277819 | — |
Reaction Steps
A solution of 3-(4,4,5,5-Tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenylamine (0.5 g, 2.28 mmol) in 2-Bromo-1-methyl-1H-imidazole (0.367 g, 2.28 mmol) was heated in a CEM discover microwave synthesizer (50 W) at 125° C. until the reaction was complete. The reaction mixture was cooled and used directly in the next procedure. MS: [M+H]+ 300
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08513276B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-084efd0076104a4aa353ffb5a78ae366 |
| Source note | uspto-grants-2013_08 |