HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl acetone → 4-[2-(4-Phenylbutan-2-ylidene)hydrazinyl]pyridin-2(1H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl acetone | HCID 17355 | — |
| Reactant | 4-Hydrazinylpyridin-2(1H)-one | HCID 13610829 | — |
| Product | 4-[2-(4-Phenylbutan-2-ylidene)hydrazinyl]pyridin-2(1H)-one | HCID 71412049 | — |
Reaction Steps
In accordance with the same procedures as in Step 2 of Preparation 1, except for using 4-hydrazino-1H-pyridin-2-one (5.39 g, 43.1 mmol) prepared in Step 1 of Preparation 1 and benzylacetone (9.70 ml, 64.6 mmol), the titled compound was obtained as a white solid. (Yield: 66.5%) The product was used in the subsequent reaction without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08513277B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-1b438df3be1b489e8f7355d249524fbe |
| Source note | uspto-grants-2013_08 |