HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Hexene-2-one → HCID 86663147, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Hexene-2-one | HCID 7989 | — |
| Reactant | 4-Hydrazinylpyridin-2(1H)-one | HCID 13610829 | — |
| Product | HCID 86663147 | HCID 86663147 | 71.3% |
Reaction Steps
In accordance with the same procedures as in Step 2 of Preparation 1, except for using 4-hydrazino-1H-pyridin-2-one (5.39 g, 43.1 mmol) prepared in Step 1 of Preparation 1 and 5-hexen-2-one (7.41 ml, 64.6 mmol), the titled compound was obtained as a white solid. (Yield: 71.3%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08513277B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-b7dfcde17a2445578b92531429943991 |
| Source note | uspto-grants-2013_08 |