HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3-(Methylsulfonyl)propyl)piperazine → HCID 25262284, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3-(Methylsulfonyl)propyl)piperazine | HCID 49853478 | — |
| Reactant | HCID 131730819 | HCID 131730819 | — |
| Product | HCID 25262284 | HCID 25262284 | — |
Reaction Steps
In a manner analogous to the method described in examples 3, rac-(4S*,5R*)-4,5-bis-(4-chloro-phenyl)-2-(3,6-dimethoxy-pyridazin-4-yl)-4,5-dimethyl-4,5-dihydro-imidazole-1-carbonyl chloride was coupled with 4-[3-(methylsulfonyl)propyl]-piperazine (prepared as described in Fotouhi, N. et al. WO 2005110996) to give the title compound. HR-MS (ES, m/z) calculated for C32H39Cl2N6O5S [(M+H)+] 689.2074, observed 689.2079.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08513239B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-176000bc959642afaeb8b2177e7d14b2 |
| Source note | uspto-grants-2013_08 |