HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67646998, compound → 3-(1-(BOC-amino)-1-cyclopropyl-methyl)pyrrolidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67646998 | HCID 67646998 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-(1-(BOC-amino)-1-cyclopropyl-methyl)pyrrolidine | HCID 19691472 | 35.1% |
Reaction Steps
A sample (548 mg) of the compound from step 470d was dissolved in methanol, 140 mg of 10% Pd/C was added, and the mixture was hydrogenated at 4 atm H2 for 42 hours at room temperature. The solution was filtered, and the solvent was removed to give 140 mg of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05726182 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-599ef965de604788a8f4493886ac4c46 |
| Source note | uspto-grants-1998_03 |