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HRID1895956

反应详情

EQUATION

反应方程式

HRID 1895956 的结构方程式

REACTANTS

反应物

3
结构：Ic1ccccn1
HCID221126

2-iodo-pyridine

C5H4IN

结构：CCOP(=O)(CC#C[Si](C)(C)C)OCC
HCID10933869

未命名化合物

结构：C#CC=C1CCN(c2ncccc2[N+](=O)[O-])CC1
HCID86627335

未命名化合物

PRODUCTS

生成物

1
结构：O=[N+]([O-])c1cccnc1N1CCC(=CC#Cc2ccccn2)CC1
HCID86627336

未命名化合物

PROCEDURE

实验过程

The title compound was obtained as described for the Compound of Example 1, reacting Compound 1c with 2-iodopyridine instead of 2-bromo-6-methylpyridine. The crude was purified by flash chromatography (EtOAc—Petroleum Ether 1:1) affording the title compound.

WORKUP

后处理

  1. customThe crude was purified by flash chromatography (EtOAc—Petroleum Ether 1:1)