Phenyl isocyanate → HCID 25183674, 화합물

HRID 1895958노트

반응식

HRID 1895958 반응식
[CH3:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([C:8]#[C:9][CH:10]=[C:11]2[CH2:16][CH2:15][NH:14][CH2:13][CH2:12]2)[N:3]=1.[C:17]1([N:23]=[C:24]=[O:25])[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>C(Cl)Cl>[CH3:1][C:2]1[N:3]=[C:4]([C:8]#[C:9][CH:10]=[C:11]2[CH2:12][CH2:13][N:14]([C:24]([NH:23][C:17]3[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=3)=[O:25])[CH2:15][CH2:16]2)[CH:5]=[CH:6][CH:7]=1

참가 물질

4

반응물 2

HCID 7672Phenyl isocyanateHCID 875504022-Methyl-6-(3-piperidin-4-ylideneprop-1-ynyl)pyridine

생성물 1

HCID 25183674HCID 25183674, 화합물

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

To a solution of the Compound of Example 3 (0.11 g, 0.52 mmol) in CH2Cl2 (10 mL) was added phenylisocyanate (0.06 mL, 0.54 mmol) and the reaction mixture was stirred overnight at r.t.

출처 및 근거

ORD 기록
ord-8439931f541d49f7bfe2494a238be061
출처 데이터셋
uspto-grants-2013_08
특허 번호
US08518916B2

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