HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Phenyl isocyanate → 4-[3-(6-methylpyridin-2-yl)prop-2-ynylidene]-N-phenylpiperidine-1-carboxamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Phenyl isocyanate | HCID 7672 | — |
| Edukt | 2-Methyl-6-(3-piperidin-4-ylideneprop-1-ynyl)pyridine | HCID 87550402 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | 4-[3-(6-methylpyridin-2-yl)prop-2-ynylidene]-N-phenylpiperidine-1-carboxamide | HCID 25183674 | — |
Reaktionsschritte
To a solution of the Compound of Example 3 (0.11 g, 0.52 mmol) in CH2Cl2 (10 mL) was added phenylisocyanate (0.06 mL, 0.54 mmol) and the reaction mixture was stirred overnight at r.t.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08518916B2 |
| Quelldatensatz | uspto-grants-2013_08 |
| ORD ID | ord-8439931f541d49f7bfe2494a238be061 |
| Quellennotiz | uspto-grants-2013_08 |