HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-3-nitropyridine → HCID 68723887, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-3-nitropyridine | HCID 79613 | — |
| Reactant | HCID 68976689 | HCID 68976689 | — |
| Product | HCID 68723887 | HCID 68723887 | 54.1% |
Reaction Steps
A well homogenised mixture of Compound 31a (24 mg, 0.11 mmol) and 2-chloro-3-nitropyridine (19.5 mg, 0.12 mmol) was stirred at 120° C. for 40 min. The reaction crude was purified by flash chromatography (EtOAc—Petroleum Ether 3:7) affording the title product (20 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08518916B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-983693ba9e0141c4a06cb15e62ade052 |
| Source note | uspto-grants-2013_08 |