huagongshe.com
HRID1895967

反应详情

EQUATION

反应方程式

HRID 1895967 的结构方程式

REACTANTS

反应物

2
结构：N#Cc1ccncc1Br
HCID11074051

3-Bromo-4-cyanopyridine

C6H3BrN2

结构：CC(C)(C)OC(=O)N1CCC(=CC#Cc2cncc(C#N)c2)CC1
HCID25183829

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N1CCC(=CC#Cc2ccc(C#N)nc2)CC1
HCID87550158

未命名化合物

PROCEDURE

实验过程

The title compound was prepared following the procedure described for the compound of Example 45, but substituting 5-bromo-2-pyridincarbonitrile for 5-bromoisonicotinonitrile. Purification by flash chromatography (EtOAc—Petroleum Ether gradient from 5:95 to 40:60) afforded the title product.

WORKUP

后处理

  1. customThe title compound was prepared
  2. customPurification by flash chromatography (EtOAc—Petroleum Ether gradient from 5:95 to 40:60)