HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-6-methyl-3-nitropyridine → HCID 68724968, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-6-methyl-3-nitropyridine | HCID 1268230 | — |
| Reactant | HCID 68976689 | HCID 68976689 | — |
| Product | HCID 68724968 | HCID 68724968 | — |
Reaction Steps
The title compound was prepared following the procedure described for the Compound of Example 31, using 2-chloro-3-nitro-6-picoline instead of 2-bromo-3-nitropyridine. The crude was purified by automated flash liquid chromatography (Horizon™-Biotage) eluting with Petroleum Ether/EtOAc 7:3, affording the title product as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08518916B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-251a297bc95c45a6912ddd98af5dd4ce |
| Source note | uspto-grants-2013_08 |