Pyridinium chloride → HCID 10483384, compound

Participants

Reaction Steps

2-[4-[2-(benzothiazol-2-ylthio)ethyl]piperazin-1-yl]-N-[2,6-dimethyl-4-trifluoromethyl-3-pyridyl]acetamide (500 mg, 0.98 mmol) was dissolved in ethanol (10 mL), followed by the addition of pyridine hydrochloride (227 mg, 1.96 mmol). The reaction mixture was concentrated, and to the residue, ethanol (0.2 mL) and water (2 mL) were added. A precipitate was collected by filtration to obtain the title compound (295 mg, 55%) as a colorless crystalline powder.

Provenance & Evidence