反应详情

温度

80 °C

To neat propargyl alcohol (1 mL) were added tributyltin hydride (5.8 mL) followed by 1,1′-azobis(cyclohexanecarbonitrile) (213 mg). The mixture was heated for 2 h at 80° C., cooled to RT and directly purified by CC (EA/Hept 4/96 to 5/95) to afford the desired compound (2.98 g).

1. temperaturecooled to RT
2. customdirectly purified by CC (EA/Hept 4/96 to 5/95)