HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 50995660, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Ethyl 3-(pyridin-3-yl)butanoate | HCID 12727116 | — |
| Product | HCID 50995660 | HCID 50995660 | 47% |
Reaction Steps
A solution of ethyl 3-(pyridin-3-yl)butanoate (0.50 g, 2.59 mmol) in methanolic ammonia (10 ml) was heated to 100° C. in a pressure bomb overnight. The solvent was evaporated under reduced pressure, washed with n-pentane and dried under reduced pressure to afford 0.2 g (47%) of 3-(pyridin-3-yl)butanamide as pale brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08518948B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-fca5c3c5070245c3a401fb50552faf49 |
| Source note | uspto-grants-2013_08 |