HuagongsheHuagongshe Chemistry Print Report · For research reference only
Malonic Acid → HCID 14994646, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Malonic Acid | HCID 867 | — |
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | 1-Benzothiophene-2-carbaldehyde | HCID 736500 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 14994646 | HCID 14994646 | — |
Reaction Steps
To a mixture of 1-benzothiophene-2-carbaldehyde, malonic acid (1.5 equiv) and pyridine (2.5 equiv) was added piperidine (0.1 equiv). The mixture was heated to reflux for 6 h, cooled and poured into H2O and filtered. Air drying over night gave the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08518964B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-6d110ac8a16c4fd99eb7e51b3264e27a |
| Source note | uspto-grants-2013_08 |